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A chemometric-assisted method for automatic, rapid and non-targeted detection of multi-pesticides in plant-derived foods by gas chromatography-mass spectrometry

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文献类型：外文期刊

作者： Su, Guanglin ¹ ; Xie, Shue ³ ; Jiang, Liwen ¹ ; Du, Guorong ¹ ; Li, Pao ¹ ;

作者机构： 1.Hunan Agr Univ, Coll Food Sci & Technol, Changsha 410128, Peoples R China

2.Hunan Acad Agr Sci, Hunan Agr Prod Proc Inst, Changsha 410125, Peoples R China

3.Hunan Prov Inst Qual Supervis & Inspect Prod, Changsha 410007, Peoples R China

4.Shanghai Tobacco Grp Co Ltd, Beijing Work Stn, Technol Ctr, Beijing 101121, Peoples R China

5.Shaoguan Univ, Guangdong Prov Key Lab Utilizat & Conservat Food &, Shaoguan 512005, Peoples R China

关键词： Multi -pesticide; Plant -derived foods; Non -targeted detection; Gas chromatography-mass spectrometry; Chemometrics

期刊名称：FOOD CHEMISTRY （影响因子：8.8；五年影响因子：8.6 ）

ISSN： 0308-8146

年卷期： 2024 年 443 卷

页码：

收录情况： SCI

摘要： An automatic, rapid and non-targeted detection method for multi-pesticides in plant-derived foods was developed by gas chromatography-mass spectrometry and chemometrics. In this method, a novel algorithm named moving window iterative target transformation factor analysis was proposed. Although there are challenges of peak overlapping and background interference, the retention time and corrected mass spectra of unknown pesticides can be automatically obtained through iteration calculation in the 'moving window' with reference to the pesticide mass spectral library. One mixed pesticide standard and nine varieties of plant-derived foods were investigated with the proposed method. By contrast, a fast temperature programme was used to shorten detection time compared to the standard temperature programme. For the mixed standard, the mass spectra and retention times of all 39 pesticides were successfully obtained from the overlapping signal. Furthermore, all spiked pesticides were successfully detected in plant-derived foods within 10 min using a fast temperature programme.

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